Available Instruments
- TGA - Thermogravimetric Analysis
Equipment
![](http://sites.fct.unl.pt/labanalises/files/tga.png)
Thermogravimetric Analyzer Setaram Labsys EVO. This equipment works in the temperature range between room temperature and 1600 °C, the heating and cooling speeds are between 0,01 an 100 °C / min. Weighing precision of +/-0,01%.
Samples
Homogenous solid or liquid samples with a minimum of 10 mg.
- DSC - Differential Scanning Calorimetry
Equipment
![](https://sites.fct.unl.pt/sites/default/files/imagecache/inline_larger/labanalises/files/dsc.png)
DSC 131, Setaram, France.
This equipment works in the temperature range between -150° and +550 °C, the heating and cooling speeds between 0,001 and 50°C / min. The sign of heat flux ranges from -100 to +100 mW and the resolution is ± 0,2 μW.
Samples
Homogenous solid or liquid samples with a minimum of 10 mg.
- XRPD - X-Ray Powder Difraction
Equipment
![](http://sites.fct.unl.pt/labanalises/files/xrpd.png)
Benchtop X-Ray Diffractometer RIGAKU, model MiniFlex II with:
Cu X-ray tube (30KV/15 mA) Scanning range: 3~ +145° (2θ)
Scanning speed: 0,01~ +100°/min (2θ)
Minimum step width: 0,01° (2θ).
Samples
Samples in dry powder form and homogeneous. The samples should be supplied in sufficient amount to cover 2 cm2 of the sample plate.
- FT-IR - Fourier Transform Infrared Spectroscopy
Equipment
![](http://sites.fct.unl.pt/labanalises/files/ftir.png)
FT-IR Spectrometer, Perkin-Elmer - Spectrum Two.
Samples
Liquids or dry solids.
- MIP - Mercury Intrusion Porosimetry
Equipment
![](http://sites.fct.unl.pt/labanalises/files/porosimetria_hg.png)
Mercury porosimeter Micromeritics Autopore IV 9500.
Sample
Dry solids. The block-shaped materials have to be adaptable to the 3, 5 or 15 cm3 penetrometers. Samples cannot form amalgams with mercury.
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ASAP - Gas Porosimetry - Nitrogen
Equipment
![](http://sites.fct.unl.pt/labanalises/files/asap.png)
Gas porosimeter Micromeritics ASAP 2010 (Accelerated Surface Area and Porosimetry System).
Sample
Dry solids. Must be delivered at least 100 mg of sample.
Application forms download
Prices